EuWO4(OH) nanobelts were synthesized for the first time via a thiourea-assisted hydrothermal reaction. The nanobelts were further hybridized with Au nanoparticles (NPs) and showed excellent performance in H2O2 detection, due to both the enzyme-mimic catalytic properties of Au NPs and the radical responsive -OH groups on the EuWO4(OH) nanobelt surfaces.