Cross-Metathesis Approach to the Tricyclic Marine Alkaloids (-)-Fasicularin and (-)-Lepadiformine A

J Org Chem. 2017 Aug 18;82(16):8497-8505. doi: 10.1021/acs.joc.7b01135. Epub 2017 Aug 8.

Abstract

A cross-metathesis protocol has been developed to provide facile access to highly hindered trisubstituted α-branched olefins, which when coupled with a cationic azaspirocyclization reaction, generates the marine alkaloids (-)-fasicularin 2 and a pro-forma synthesis of (-)-lepadiformine A 1.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Alkaloids / chemical synthesis*
  • Alkaloids / chemistry
  • Molecular Structure
  • Thiocyanates / chemical synthesis*
  • Thiocyanates / chemistry

Substances

  • Alkaloids
  • Thiocyanates
  • fasicularin
  • lepadiformine