Isosorbide-based peptidomimetics as inhibitors of hepatitis C virus serine protease

Bioorg Med Chem Lett. 2017 Aug 15;27(16):3661-3665. doi: 10.1016/j.bmcl.2017.07.027. Epub 2017 Jul 8.

Abstract

Hepatitis C infection is a cause of chronic liver diseases such as cirrhosis and carcinoma. The current therapy for hepatitis C has limited efficacy and low tolerance. The HCV encodes a serine protease which is critical for viral replication, and few protease inhibitors are currently on the market. In this paper, we describe the synthesis and screening of novel isosorbide-based peptidomimetic inhibitors, in which the compounds 1d, 1e, and 1i showed significant inhibition of the protease activity in vitro at 100µM. The compound 1e also showed dose-response (IC50=36±3µM) and inhibited the protease mutants D168A and V170A at 100µM, indicating it as a promising inhibitor of the HCV NS3/4A protease. Our molecular modeling studies suggest that the activity of 1e is associated with a change in the interactions of S2 and S4 subsites, since that the increased flexibility favors a decrease in activity against D168A, whereas the appearance of a hydrophobic cavity in the S4 subsite increase the inhibition against V170A strain.

Keywords: HCV; Isosorbide; MMPBSA; Molecular docking; Molecular dynamic simulation; Peptidomimetics; Serine proteases.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Antiviral Agents / chemical synthesis
  • Antiviral Agents / chemistry*
  • Antiviral Agents / pharmacology
  • Binding Sites
  • Catalytic Domain
  • Hepacivirus / drug effects
  • Hepacivirus / enzymology*
  • Isosorbide / chemical synthesis
  • Isosorbide / chemistry*
  • Isosorbide / pharmacology
  • Molecular Docking Simulation
  • Mutation
  • Peptidomimetics
  • Serine Proteases / chemistry*
  • Serine Proteases / genetics
  • Serine Proteases / metabolism
  • Serine Proteinase Inhibitors / chemical synthesis
  • Serine Proteinase Inhibitors / chemistry*
  • Serine Proteinase Inhibitors / pharmacology
  • Thermodynamics
  • Viral Nonstructural Proteins / antagonists & inhibitors
  • Viral Nonstructural Proteins / genetics
  • Viral Nonstructural Proteins / metabolism

Substances

  • Antiviral Agents
  • NS3 protein, hepatitis C virus
  • NS4 protein, hepatitis C virus
  • Peptidomimetics
  • Serine Proteinase Inhibitors
  • Viral Nonstructural Proteins
  • Serine Proteases
  • Isosorbide