A dual-label time-resolved fluorescence immunoassay for the simultaneous determination of cystatin C and β2-microglobulin in urine

Br J Biomed Sci. 2017 Oct;74(4):193-197. doi: 10.1080/09674845.2017.1334740. Epub 2017 Jul 21.

Abstract

Background: Contrast media is widely used in clinical diagnostic and interventional procedures, but may cause damage to the kidney, that is, contrast-induced nephropathy. This study was to establish a dual-label time-resolved fluorescence immunoassay (TRFIA) for the simultaneous determination of renal function markers cystatin-C (Cys-C) and β2-microglobulin (β2-MG) for the early diagnosis and follow-up surveillance of contrast-induced nephropathy.

Methods: A sandwich immunoassay was used to detect the concentration of Cys-C, and the competitive immunoassay was used to detect the concentration of β2-MG in 50 samples of urine. The performance of this dual-label TRFIA was evaluated and compared with commercial assays.

Results: The sensitivity for Cys-C detection was 1.26 ng/ml, the average recovery was 99.36%; The sensitivity for β2-MG detection was 2.13 ng/ml, the average recovery was 100.18%. Bland-Altman analysis showed that the dual-label TRFIA method and the commercial kits had a good agreement, suggesting they can be used interchangeably in clinical urine analysis.

Conclusion: The present dual-label TRFIA has high sensitivity, specificity and accuracy in clinical sample analysis. This method can be used for the early diagnosis and follow-up surveillance of the contrast-induced nephropathy.

Keywords: Contrast-induced nephropathy; cystatin-C; dual-label time-resolved fluorescence immunoassay; β2-microglobulin.

MeSH terms

  • Cystatin C / urine*
  • Female
  • Fluorescence
  • Fluoroimmunoassay / methods*
  • Humans
  • Male
  • Middle Aged
  • Reference Standards
  • Time Factors
  • beta 2-Microglobulin / urine*

Substances

  • Cystatin C
  • beta 2-Microglobulin