Artificial β-Double Helices from Achiral γ-Peptides

Angew Chem Int Ed Engl. 2018 Jan 22;57(4):1057-1061. doi: 10.1002/anie.201711124. Epub 2017 Dec 27.

Abstract

Double helices are not common in polypeptides and proteins except in the peptide antibiotic gramicidin A and analogous l,d-peptides. In contrast to natural polypeptides, remarkable β-double-helical structures from achiral γ-peptides built from α,β-unsaturated γ-amino acids have been observed. The crystal structures suggest that they adopted parallel β-double helical structures and these structures are stabilized by the interstrand backbone amide H-bonds. Furthermore, both NMR spectroscopy and fluorescence studies support the existence of double-helical conformations in solution. Although a variety of folded architectures featuring distinct H-bonds have been discovered from the β- and γ-peptide foldamers, this is the first report to show that achiral γ-peptides can spontaneously intertwine into β-double helical structures.

Keywords: achirality; amino acids; foldamers; peptides; β-double helix.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Crystallography, X-Ray
  • Gramicidin / chemistry
  • Hydrogen Bonding
  • Models, Molecular
  • Nuclear Magnetic Resonance, Biomolecular
  • Peptides / chemistry*
  • Protein Conformation, alpha-Helical
  • Spectrometry, Fluorescence

Substances

  • Peptides
  • Gramicidin