Cloning and Characterization of the Gene Encoding Alpha-Pinene Oxide Lyase Enzyme (Prα-POL) from Pseudomonas rhodesiae CIP 107491 and Production of the Recombinant Protein in Escherichia coli

Appl Biochem Biotechnol. 2018 Jul;185(3):676-690. doi: 10.1007/s12010-017-2685-z. Epub 2017 Dec 28.

Abstract

The alpha-pinene oxide lyase (Prα-POL) from Pseudomonas rhodesiae CIP107491 belongs to catabolic alpha-pinene degradation pathway. In this study, the gene encoding Prα-POL has been identified using mapping approach combined to inverse PCR (iPCR) strategy. The Prα-POL gene included a 609-bp open reading frame encoding 202 amino acids and giving rise to a 23.7 kDa protein, with a theoretical isoelectric point (pI) of 5.23. The amino acids sequence analysis showed homologies with those of proteins with unknown function from GammaProteobacteria group. Identification of a conserved domain in amino acid in positions 18 to 190 permitted to classify Prα-POL among the nuclear transport factor 2 (NTF2) protein superfamily. Heterologous expression of Prα-POL, both under its native form and with a histidin tag, was successfully performed in Escherichia coli, and enzymatic kinetics were analyzed. Bioconversion assay using recombinant E. coli strain allowed to reach a rate of isonovalal production per gramme of biomass about 40-fold higher than the rate obtained with P. rhodesiae.

Keywords: Alpha-pinene oxide lyase; Bioconversion; Isonovalal; Orphan enzyme; Pseudomonas.

MeSH terms

  • Aldehyde-Lyases / chemistry
  • Aldehyde-Lyases / genetics*
  • Aldehyde-Lyases / metabolism
  • Aldehydes / metabolism
  • Amino Acid Sequence
  • Bacterial Proteins / genetics
  • Base Sequence
  • Biomass
  • Cloning, Molecular*
  • Escherichia coli / genetics*
  • Genes, Bacterial*
  • Isoelectric Point
  • Kinetics
  • Monoterpenes / metabolism
  • Open Reading Frames
  • Polymerase Chain Reaction / methods
  • Pseudomonas / enzymology*
  • Pseudomonas / genetics
  • Recombinant Proteins / genetics

Substances

  • Aldehydes
  • Bacterial Proteins
  • Monoterpenes
  • Recombinant Proteins
  • isonovalal
  • Aldehyde-Lyases
  • alpha-pinene oxide lyase