Essential oils (EOs), pressurized liquid extracts (PLE) and carbon dioxide supercritical fluid extracts (SFE-CO2) from Algerian Thymus munbyanus as valuable sources of antioxidants to be used on an industrial level

Food Chem. 2018 Sep 15:260:289-298. doi: 10.1016/j.foodchem.2018.03.108. Epub 2018 Mar 30.

Abstract

The aim of this study was to demonstrate the potential of extracts from Algerian Thymus munbyanus as a valuable source of antioxidants for use on an industrial level. To this end, a study was conducted on the composition and antioxidant activities of essential oils (EOs), pressurized liquid extracts (PLE) and supercritical fluid extracts (SFE-CO2) obtained from Thymus munbyanus subsp. coloratus (TMC) and subsp. munbyanus (TMM). EOs and SFE-CO2 extracts were analysed by GC-FID and GC×GC-TOFMS revealing significant differences. A successive extraction of the solid SFE-CO2 residue by PLE extraction with solvents of increasing polarity such as acetone, ethanol and water, was carried out. The extracts were evaluated for total phenolic content by Folin-Ciocalteu assay, while the antioxidant power was assessed by DPPH, FRAP, and ORAC assays. SFE-CO2 extracts were also analysed for their tocopherol content. The antioxidant activity of PLE extracts was found to be higher than that of SFE-CO2 extracts, and this increased with solvent polarity (water > ethanol > acetone). Overall, these results support the use of T. munbyanus as a valuable source of substances to be used on an industrial level as preservative agents.

Keywords: Antioxidant; EOs; PLE; SFE-CO(2); Thymus munbyanus subsp. coloratus; Thymus munbyanus subsp. munbyanus.

MeSH terms

  • Antioxidants / chemistry
  • Antioxidants / pharmacology*
  • Carbon Dioxide / chemistry
  • Chemical Fractionation / methods
  • Chromatography, Supercritical Fluid / methods
  • Ethanol / chemistry
  • Gas Chromatography-Mass Spectrometry
  • Oils, Volatile / chemistry*
  • Oils, Volatile / pharmacology
  • Phenols / analysis
  • Plant Extracts / chemistry*
  • Plant Extracts / pharmacology
  • Solvents / chemistry
  • Thymus Plant / chemistry*

Substances

  • Antioxidants
  • Oils, Volatile
  • Phenols
  • Plant Extracts
  • Solvents
  • Carbon Dioxide
  • Ethanol