Synthesis of the Aminocyclitol Core of Jogyamycin via an Enantioselective Pd-Catalyzed Trimethylenemethane (TMM) Cycloaddition

Org Lett. 2018 Jul 6;20(13):3938-3942. doi: 10.1021/acs.orglett.8b01518. Epub 2018 Jun 25.

Abstract

The use of β-nitroenamines as a new class of acceptors in the enantioselective Pd-catalyzed trimethylenemethane cycloaddition afforded differentiated 1,2-dinitrogen bearing cyclopentanes with three contiguous stereocenters. The utility of these acceptors was demonstrated with the efficient construction of the core of jogyamycin and aminocyclopentitols. Further elaboration of the cycloadducts provided a concise synthetic approach toward joygamycin.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Catalysis
  • Cycloaddition Reaction
  • Methane / analogs & derivatives
  • Molecular Structure
  • Pactamycin / analogs & derivatives*
  • Pactamycin / chemical synthesis
  • Palladium
  • Stereoisomerism

Substances

  • jogyamycin
  • trimethylenemethane
  • Pactamycin
  • Palladium
  • Methane