Identification and biological evaluation of glycol diaryl ethers as novel anti-cancer agents through structure-based optimization of crizotinib

Chem Biol Drug Des. 2018 Dec;92(6):1972-1980. doi: 10.1111/cbdd.13368. Epub 2018 Aug 26.

Abstract

Crizotinib, a drug for anaplastic lymphoma kinase (ALK) positive and c-ros oncogene 1 receptor tyrosine kinase (ROS1) positive non-small cell lung cancer (NSCLC), was structurally optimized via a strategy of structure-based fragment replacing. Computational study showed it was beneficial for interaction of crizotinib and ALK to increase the distance between pyridyl ring and phenyl ring in crizotinib, and thus, a series of novel glycol diaryl ethers were synthesized. The in vitro anti-tumor activity of synthesized compounds was studied in NSCLC cell line H2228 and neurobalstoma cell line SH-SY5Y. Among the synthesized compounds, 9e exhibits stronger anti-cancer activity than crizotinib toward H2228 cell line with an IC50 value of 0.22 μM. Molecular docking indicated that a longer chain between pyridyl ring and phenyl ring enabled molecule to have new interaction with a neighboring small hydrophobic pocket.

Keywords: ALK; Crizotinib; NSCLC; anti-cancer; glycol diaryl ether.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Anaplastic Lymphoma Kinase / antagonists & inhibitors
  • Anaplastic Lymphoma Kinase / metabolism
  • Antineoplastic Agents / chemistry*
  • Antineoplastic Agents / metabolism
  • Antineoplastic Agents / pharmacology
  • Binding Sites
  • Cell Line, Tumor
  • Cell Proliferation / drug effects
  • Crizotinib / chemistry*
  • Crizotinib / metabolism
  • Crizotinib / pharmacology
  • Drug Design
  • Ethers / chemistry*
  • Humans
  • Molecular Docking Simulation
  • Protein Structure, Tertiary

Substances

  • Antineoplastic Agents
  • Ethers
  • Crizotinib
  • ALK protein, human
  • Anaplastic Lymphoma Kinase