Formulation Development and Characterization of Nanoemulsion-Based Formulation for Topical Delivery of Heparinoid

J Pharm Sci. 2018 Nov;107(11):2883-2890. doi: 10.1016/j.xphs.2018.07.015. Epub 2018 Jul 25.

Abstract

Heparinoid is commonly used for the treatment of superficial thrombophlebitis, a condition wherein inflammation and clotting occurs in the veins below the skin surface. However, stratum corneum is a major barrier that limits the delivery of hydrophilic heparinoid, in and across the skin. The aim of the present study was to develop a nonirritant topical formulation for heparinoid incorporating chemical penetration enhancers and investigate the delivery of heparinoid across the human epidermis using in vitro vertical Franz diffusion cells. The developed oil-in-water nanoemulsions (NEs; NE-1 and NE-2) delivered higher amount of heparinoid (91.58 ± 25.75 μg/sq.cm and 62.67 ± 5.66 μg/sq.cm, respectively) after 72 h compared with the other developed formulations, which in turn also delivered significantly higher amount compared with commercial formulations: cream (1.78 ± 0.07 μg/sq.cm), ointment (9.95 ± 4.41 μg/sq.cm), and gel (0 μg/sq.cm) (p <0.05). Transmission electron microscopy, polarizing light microscopy, and dynamic light scattering studies were performed to characterize the microstructure of these NEs with chemical enhancers. NE-1 was tested to be nonirritant with cell viability greater than 50% and a minimal release of IL-1α by using the "in vitro Epiderm tissue" model. Our results demonstrate that NE formulations represent a potential strategy for providing a localized therapy for the treatment of superficial thrombophlebitis.

Keywords: emulsion; formulation; percutaneous; permeability; permeation enhancers; skin; solubility; surfactants; transdermal; transdermal drug delivery.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Administration, Cutaneous
  • Anti-Inflammatory Agents / administration & dosage*
  • Anti-Inflammatory Agents / pharmacokinetics*
  • Drug Compounding
  • Emulsions / chemistry
  • Epidermis / metabolism*
  • Heparinoids / administration & dosage*
  • Heparinoids / pharmacokinetics*
  • Humans
  • Permeability
  • Pharmaceutical Vehicles / chemistry*
  • Skin Absorption*
  • Solubility
  • Thermodynamics

Substances

  • Anti-Inflammatory Agents
  • Emulsions
  • Heparinoids
  • Pharmaceutical Vehicles