Synthesis of Benzo[1,6]naphthyridinones Using the Catellani Reaction

Org Lett. 2018 Sep 7;20(17):5228-5232. doi: 10.1021/acs.orglett.8b02171. Epub 2018 Aug 13.

Abstract

An intramolecular version of the Catellani reaction was optimized for one-step synthesis of bulky N-substituted benzo[1,6]naphthyridinones with good to excellent yields. The optimized reaction of N-substituted o-bromobenzamides with 4-bromoquinolines features a wide substrate scope and yields of up to 98%. The employment of aryl bromides under carefully optimized conditions instead of the usual aryl iodides enhances the scope of the reaction.

Publication types

  • Research Support, Non-U.S. Gov't