Preparation and characterization of pH-sensitive nanoparticles of budesonide for the treatment of ulcerative colitis

Drug Des Devel Ther. 2018 Aug 22:12:2601-2609. doi: 10.2147/DDDT.S170676. eCollection 2018.

Abstract

Objective: The aim of this study was to develop pH sensitive nanoparticles of budesonide for the treatment of ulcerative colitis.

Methods: The NPs system was characterized by the transmission electron microscopy (TEM), particle size, drug loading and encapsulation efficiency. In addition, in vitro drug release prop-erties and pharmacokinetics were also investigated in detail. The optimized formulation was examined for its in-vivo targeting potential using 2,4,6-trinitrobenzenesulfonic acid (TNBS)-induced colitis in a rat model.

Results: Dynamic light-scattering results showed that the particle size of budesonide-Eudragit S100/poly(lactic-co-glycolic acid) nanoparticles was around 110.5 nm, with a polydispersity index of 0.098. Transmission electron microscopy images showed that BUD-ES100/PLGA NPs were spherical with uniform size and relatively smooth surfaces. In vitro release showed that BUD-ES100/PLGA NPs required minimal release of drugs during its transit in the stomach and the upper small intestine to ensure that a maximum dose reached the colon. After the pharma-codynamic treatment, the myeloperoxidase value of BUD-ES100/PLGA NPs was close to the normal group. The histopathological examination of rectum showed that no sign of damages such as epithelial necrosis and sloughing epithelial cells was detected.

Conclusion: Our findings suggested that BUD-ES100/PLGA NPs were a promising alternative to single pH-dependent systems for colitis therapy.

Keywords: ES100/PLGA; budesonide; in vitro release; nanoparticles; pharmacodynamic.

MeSH terms

  • Animals
  • Anti-Inflammatory Agents / administration & dosage*
  • Anti-Inflammatory Agents / chemical synthesis
  • Anti-Inflammatory Agents / chemistry
  • Anti-Inflammatory Agents / therapeutic use*
  • Budesonide / administration & dosage*
  • Budesonide / chemical synthesis
  • Budesonide / chemistry
  • Budesonide / therapeutic use*
  • Colitis, Ulcerative / chemically induced
  • Colitis, Ulcerative / drug therapy*
  • Disease Models, Animal
  • Humans
  • Hydrogen-Ion Concentration
  • Mice
  • Mice, Inbred Strains
  • Nanoparticles / chemistry*
  • Trinitrobenzenesulfonic Acid

Substances

  • Anti-Inflammatory Agents
  • Budesonide
  • Trinitrobenzenesulfonic Acid