Biofilm Inhibitory Abscisic Acid Derivatives from the Plant-Associated Dothideomycete Fungus, Roussoella sp

Molecules. 2018 Aug 30;23(9):2190. doi: 10.3390/molecules23092190.

Abstract

Roussoella species are well recorded from both monocotyledons and dicotyledons. As part of a research program to discover biologically active compounds from plant-associated Dothideomycetes in Thailand, the strain Roussoella sp. (MFLUCC 17-2059), which represents an undescribed species, was isolated from Clematis subumbellata Kurz, fermented in yeast-malt medium and explored for its secondary metabolite production. Bioassay-guided fractionation of the crude extract yielded the new abscisic acid derivative, roussoellenic acid (1), along with pestabacillin B (2), a related congener, and the cyclodipeptide, cyclo(S-Pro-S-Ile) (3). The structure of 1 was determined by 2D NMR spectroscopy and HR-ESIMS data analysis. Compounds 1 and 2 showed inhibitory activity on biofilm formation by Staphylococcus aureus. The biofilm formation of S. aureus was reduced to 34% at 16 µg/mL by roussoellenic acid (1), while pestabacillin B (2) only showed 36% inhibition at 256 µg/mL. In addition, compound 1 also had weak cytotoxic effects on L929 murine fibroblasts and human KB3-1 cancer cells.

Keywords: Anti-biofilm; Ascomycota; Pleosporales; structure elucidation.

MeSH terms

  • Abscisic Acid / analogs & derivatives
  • Abscisic Acid / chemistry
  • Abscisic Acid / pharmacology*
  • Anti-Infective Agents / chemistry
  • Anti-Infective Agents / pharmacology*
  • Ascomycota / chemistry
  • Ascomycota / genetics*
  • Biofilms / drug effects*
  • Biological Products / chemistry
  • Biological Products / pharmacology*
  • Humans
  • Molecular Structure

Substances

  • Anti-Infective Agents
  • Biological Products
  • Abscisic Acid