A Novel Proof-of-Concept Sandwich Immunoassay for Screening Microcystin in Cyanobacteria Based on Michael Addition Reaction

Anal Sci. 2019 Jan 10;35(1):107-111. doi: 10.2116/analsci.18SDN03. Epub 2018 Oct 5.

Abstract

We present an innovative concept of a screening tool for detecting free microcystin in cyanobacteria using a sandwich immunodetection format, based on Michael addition reaction between α,β-unsaturated carbonyl moiety of microcystin and thiol of coating substance. This proof-of-concept immunoassay was developed using bovine serum albumin as a microcystin-binding model, and was tested with toxic Microcystis samples. The preliminary results indicate that the proposed Michael addition-based immunodetection is promising and can be used as a platform for further development to become a useful tool for free microcystin analysis in various samples in the future.

Keywords: ELISA; Michael addition reaction; Microcystin; free form; sandwich immunoassay.

MeSH terms

  • Cyanobacteria / chemistry*
  • Immunoassay / methods*
  • Microcystins / analysis*
  • Microcystis / chemistry
  • Proof of Concept Study*
  • Protein Binding
  • Reproducibility of Results
  • Sensitivity and Specificity
  • Serum Albumin, Bovine / chemistry

Substances

  • Microcystins
  • Serum Albumin, Bovine
  • microcystin