Improved Soluble Expression and Catalytic Activity of a Thermostable Esterase Using a High-Throughput Screening System Based on a Split-GFP Assembly

J Agric Food Chem. 2018 Dec 5;66(48):12756-12764. doi: 10.1021/acs.jafc.8b04646. Epub 2018 Nov 26.

Abstract

The thermostable esterase Aaeo1 displays a low expression level and forms a great amount of inclusion bodies in E. coli. Herein, a split-GFP system was established in which the fluorescence intensity exhibited a good linear correlation with the soluble protein expression level and the esterase activity. In the primary high-throughput screening, the mutant library was screened by flow cytometry via detection of a split-GFP reporter. Then, through a secondary screening against esterase activity, two mutants with improved soluble expression and catalytic activity were obtained. The soluble expression of the mutant enzymes in E. coli was improved by 2-fold. The kcat/ Km values of the mutant enzymes were 2-fold higher than that of the parent. We explored the relationship between the amino acid mutations in the two mutants and the enzyme activity. The enzyme activity of mutant I51V-E170D was 4.5 times higher than that of the parent.

Keywords: catalytic activity; high-throughput screening; soluble expression; split-GFP; thermostable esterase.

Publication types

  • Evaluation Study

MeSH terms

  • Aquifoliaceae / chemistry
  • Aquifoliaceae / enzymology*
  • Aquifoliaceae / genetics
  • Bacterial Proteins / chemistry*
  • Bacterial Proteins / genetics*
  • Bacterial Proteins / metabolism
  • Biocatalysis
  • Enzyme Stability
  • Esterases / chemistry*
  • Esterases / genetics*
  • Esterases / metabolism
  • Fluorescence
  • Gene Library
  • Genes, Reporter
  • Green Fluorescent Proteins / chemistry
  • Green Fluorescent Proteins / genetics
  • Green Fluorescent Proteins / metabolism
  • High-Throughput Screening Assays / methods*
  • Hot Temperature
  • Kinetics
  • Mutation
  • Protein Engineering
  • Solubility

Substances

  • Bacterial Proteins
  • Green Fluorescent Proteins
  • Esterases