Analyses of active antioxidant polysaccharides from four edible mushrooms

Int J Biol Macromol. 2019 Feb 15:123:945-956. doi: 10.1016/j.ijbiomac.2018.11.079. Epub 2018 Nov 15.

Abstract

Four water-soluble polysaccharides were extracted from Pleurotus eryngii, Flammulina velutipes, Pleurotus ostreatus and white Hypsizygus marmoreus. Using anion exchange and gel permeation chromatography, a neutral and an acidic fraction were purified from each water-soluble polysaccharide. Their molecular weights were all around 20 kDa except that the acidic polysaccharide from Pleurotus ostreatus (named WPOPA) had a lower molecular weight of 5 kDa. Four neutral polysaccharides were mainly composed of galactose (42.7%-69.1%), followed by Man (19.4%-39.3%) and Glc (1.1%-15.9%). Four acidic polysaccharides contained glucose (59.0%-81.8%) as major sugar and minor glucuronic acid (4.5%-9.5%). Acidic polysaccharides exhibited stronger antioxidant activities than neutral fractions, and WPOPA showed the best antioxidant effects. Structural analysis indicated WPOPA had β-(1 → 6)-glucan backbone branched at O-3 by β-1,3-d-Glcp, t-β-d-Glcp and t-β-d-GlcpA. This investigation would be useful for screening natural antioxidants and significant in developing mushroom polysaccharides as functional foods.

Keywords: Antioxidant activities; Mushroom polysaccharides; Structural characterization.

MeSH terms

  • Agaricales / chemistry*
  • Antioxidants / analysis*
  • Carbon-13 Magnetic Resonance Spectroscopy
  • Chemical Fractionation
  • Glucuronic Acid / analysis
  • Hydrolysis
  • Methylation
  • Molecular Weight
  • Oxidation-Reduction
  • Polysaccharides / analysis*
  • Polysaccharides / chemistry
  • Polysaccharides / isolation & purification
  • Spectroscopy, Fourier Transform Infrared

Substances

  • Antioxidants
  • Polysaccharides
  • Glucuronic Acid