Discovery of novel simplified isoxazole derivatives of sampangine as potent anti-cryptococcal agents

Bioorg Med Chem. 2019 Mar 1;27(5):832-840. doi: 10.1016/j.bmc.2019.01.029. Epub 2019 Jan 25.

Abstract

Cryptococcus neoformans is the leading cause of cryptococcal meningitis, which is associated with high mortality due to lack of effective treatment. Herein a series of tricyclic isoxazole derivatives with excellent anti-cryptococcal activities were identified by structural simplification and scaffold hopping of antifungal natural product sampangine. Particularly, compound 8a showed promising features as an anti-cryptococcal lead compound. It was highly active against C. neoformans (MIC80 = 0.031 μg/mL), which was more potent than fluconazole and voriconazole. Moreover, compound 8a showed potent fungicidal activity and had potent inhibitory effects against important virulence factors (i.e. biofilm, melanin and urease) of C. neoformans. Preliminary antifungal mechanism investigation revealed that compound 8a induced apoptosis of C. neoformans cells and arrested the cell cycle at the G1/S phase.

Keywords: Anti-cryptococcal; Antifungal mechanism; Fungicidal activity; Structural simplification; Virulence factors.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Alkaloids / chemical synthesis
  • Alkaloids / chemistry
  • Alkaloids / pharmacology*
  • Antifungal Agents / chemical synthesis
  • Antifungal Agents / chemistry
  • Antifungal Agents / pharmacology*
  • Apoptosis / drug effects
  • Biofilms / drug effects
  • Cryptococcus neoformans / drug effects*
  • Drug Discovery
  • G1 Phase Cell Cycle Checkpoints / drug effects
  • Heterocyclic Compounds, 4 or More Rings / chemical synthesis
  • Heterocyclic Compounds, 4 or More Rings / chemistry
  • Heterocyclic Compounds, 4 or More Rings / pharmacology*
  • Isoxazoles / chemical synthesis
  • Isoxazoles / chemistry
  • Isoxazoles / pharmacology*
  • Melanins / antagonists & inhibitors
  • Microbial Sensitivity Tests
  • Molecular Structure
  • Naphthyridines / chemical synthesis
  • Naphthyridines / chemistry
  • Naphthyridines / pharmacology*
  • Structure-Activity Relationship
  • Urease / antagonists & inhibitors

Substances

  • Alkaloids
  • Antifungal Agents
  • Heterocyclic Compounds, 4 or More Rings
  • Isoxazoles
  • Melanins
  • Naphthyridines
  • Urease
  • sampangine