Synthesis of Benz-Fused Azoles via C-Heteroatom Coupling Reactions Catalyzed by Cu(I) in the Presence of Glycosyltriazole Ligands

ACS Comb Sci. 2019 May 13;21(5):389-399. doi: 10.1021/acscombsci.9b00004. Epub 2019 Apr 16.

Abstract

Glycosyl triazoles are conveniently accessible and contain multiple metal-binding units that may assist in metal-mediated catalysis. Azide derivatives of d-glucose have been converted to their respective aryltriazoles and screened as ligands for the synthesis of 2-substituted benz-fused azoles and benzimidazoquinazolinones by Cu-catalyzed intramolecular Ullmann type C-heteroatom coupling. Good to excellent yields for a variety of benz-fused heterocyles were obtained for this readily accessible catalytic system.

Keywords: benzazole; catalysis; click chemistry; cross-coupling; glycosyl triazole; ligand.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Azides / chemistry
  • Azoles / chemical synthesis*
  • Catalysis
  • Copper / chemistry*
  • Glycosylation
  • Ligands
  • Molecular Structure
  • Quinazolinones / chemistry
  • Triazoles / chemistry

Substances

  • Azides
  • Azoles
  • Ligands
  • Quinazolinones
  • Triazoles
  • Copper