Synthesis of benzoxazoles via the copper-catalyzed hydroamination of alkynones with 2-aminophenols

Org Biomol Chem. 2019 Apr 24;17(17):4225-4229. doi: 10.1039/c9ob00572b.

Abstract

We describe herein the synthetic method to benzoxazole derivatives via the copper-catalyzed hydroamination of alkynones with 2-aminophenols. The method produced a wide variety of functionalized benzoxazole derivatives in good yields. Preliminary mechanistic experiments revealed that the reaction would proceed through the copper-catalyzed hydroamination of alkynones and the sequential intramolecular cyclization of β-iminoketones/elimination of acetophenone promoted by the copper catalyst.

Publication types

  • Research Support, Non-U.S. Gov't