Dendrimer Conjugation Enables Multiphoton Chemical Neurophysiology Studies with an Extended π-Electron Caging Chromophore

Angew Chem Int Ed Engl. 2019 Aug 26;58(35):12086-12090. doi: 10.1002/anie.201906067. Epub 2019 Jul 19.

Abstract

We have developed a caged neurotransmitter using an extended π-electron chromophore for efficient multiphoton uncaging on living neurons. Widely studied in a chemical context, such chromophores are inherently bioincompatible due to their highly lipophilic character. Attachment of two polycarboxylate dendrimers, a method we call "cloaking", to a bisstyrylthiophene (or BIST) core effectively transformed the chromophore into a water-soluble optical probe, whilst maintaining the high two-photon absorption of over 500 GM. Importantly, the cloaked caged compound was biologically inert at the high concentrations required for multiphoton chemical physiology. Thus, in contrast to non-cloaked BIST compounds, the BIST-caged neurotransmitter can be safely delivered onto neurons in acutely isolated brain slices, thereby enabling high-resolution two-photon uncaging without any side effects. We expect that our cloaking method will enable the development of new classes of cell-compatible photolabile probes using a wide variety of extended π-electron caging chromophores.

Keywords: caged compounds; dendrimers; neurophysiology; photopharmacology; two-photon uncaging.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Dendrimers / chemistry*
  • Dendrimers / metabolism
  • Electrons
  • Induced Pluripotent Stem Cells / cytology
  • Induced Pluripotent Stem Cells / metabolism
  • Mice
  • Neurons / metabolism
  • Neurotransmitter Agents / chemistry
  • Neurotransmitter Agents / metabolism
  • Photons
  • Thiophenes / chemistry
  • gamma-Aminobutyric Acid / chemistry
  • gamma-Aminobutyric Acid / metabolism

Substances

  • Dendrimers
  • Neurotransmitter Agents
  • Thiophenes
  • gamma-Aminobutyric Acid