Design, synthesis and evaluation of biphenyl imidazole analogues as potent antifungal agents

Bioorg Med Chem Lett. 2019 Sep 1;29(17):2448-2451. doi: 10.1016/j.bmcl.2019.07.037. Epub 2019 Jul 23.

Abstract

To further explore the structure activity relationships (SARs) of our previously discovered antifungal lead compound (1), a series of biphenyl imidazole analogues were designed, synthesized and evaluated for their in vitro antifungal activity. Many of the synthesized compounds showed excellent activity against Candida albicans and Candida tropicalis. Among these compounds, 2-F substituted analogue 12m displayed the most remarkable in vitro activity against C. albicans, C. neoformans, A. fumigatus and fluconazole-resistant C. alb. strains, which is superior or comparable to the activity of the reference drugs fluconazole and itraconazole. Notably, the compound 12m exhibited low inhibition profiles for various human cytochrome P450 isoforms and showed low toxicity to mammalian A549 cells and U87 cells. The SARs and binding mode established in this study will be useful for further lead optimization.

Keywords: Antifungal activity; Azole antifungals; CYP51; Structure-activity relationship.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Antifungal Agents / chemical synthesis*
  • Antifungal Agents / pharmacology
  • Aspergillus fumigatus / drug effects
  • Binding Sites
  • Biphenyl Compounds / chemistry
  • Candida albicans / drug effects
  • Catalytic Domain
  • Cell Line, Tumor
  • Cell Survival / drug effects
  • Cytochrome P-450 Enzyme System / chemistry
  • Cytochrome P-450 Enzyme System / metabolism
  • Drug Design*
  • Fluconazole / pharmacology
  • Fungal Proteins / antagonists & inhibitors
  • Fungal Proteins / metabolism
  • Humans
  • Imidazoles / chemistry*
  • Imidazoles / pharmacology
  • Microbial Sensitivity Tests
  • Molecular Docking Simulation
  • Protein Isoforms / antagonists & inhibitors
  • Protein Isoforms / metabolism
  • Structure-Activity Relationship

Substances

  • Antifungal Agents
  • Biphenyl Compounds
  • Fungal Proteins
  • Imidazoles
  • Protein Isoforms
  • biphenyl
  • Fluconazole
  • Cytochrome P-450 Enzyme System