Exploring benzoxaborole derivatives as carbonic anhydrase inhibitors: a structural and computational analysis reveals their conformational variability as a tool to increase enzyme selectivity

J Enzyme Inhib Med Chem. 2019 Dec;34(1):1498-1505. doi: 10.1080/14756366.2019.1653291.

Abstract

Recent studies identified the benzoxaborole moiety as a new zinc-binding group able to interact with carbonic anhydrase (CA) active site. Here, we report a structural analysis of benzoxaboroles containing urea/thiourea groups, showing that these molecules are very versatile since they can bind the enzyme assuming different binding conformations and coordination geometries of the catalytic zinc ion. In addition, theoretical calculations of binding free energy were performed highlighting the key role of specific residues for protein-inhibitor recognition. Overall, these data are very useful for the development of new inhibitors with higher selectivity and efficacy for various CAs.

Keywords: Carbonic anhydrase inhibitors; X-ray crystallography; benzoxaborole derivatives; binding free energy calculations; structure-based drug design.

MeSH terms

  • Boron Compounds / chemical synthesis
  • Boron Compounds / chemistry
  • Boron Compounds / pharmacology*
  • Carbonic Anhydrase Inhibitors / chemical synthesis
  • Carbonic Anhydrase Inhibitors / chemistry
  • Carbonic Anhydrase Inhibitors / pharmacology*
  • Carbonic Anhydrases / metabolism*
  • Crystallography, X-Ray
  • Dose-Response Relationship, Drug
  • Humans
  • Models, Molecular
  • Molecular Conformation
  • Structure-Activity Relationship

Substances

  • Boron Compounds
  • Carbonic Anhydrase Inhibitors
  • Carbonic Anhydrases

Grants and funding

This work is supported by the Italian Ministero dell'Istruzione, dell'Università e della Ricerca (MIUR), through the Programmi di Ricerca di Rilevante Interesse Nazionale (PRIN) Project 201744BN5T and by Regione Campania through the PO FESR 2014–2020 “eMORFORAD”.