Thermoresponsive in Situ Forming Hydrogel with Sol-Gel Irreversibility for Effective Methicillin-Resistant Staphylococcus aureus Infected Wound Healing

ACS Nano. 2019 Sep 24;13(9):10074-10084. doi: 10.1021/acsnano.9b02845. Epub 2019 Aug 27.

Abstract

An in situ forming hydrogel has emerged as a promising wound dressing recently. As physically cross-linked hydrogels are normally unstable, most in situ forming hydrogels are chemically cross-linked. However, big concerns have remained regarding the slow gelation and the potential toxicity of residual functional groups from cross-linkers or the polymer matrix. Herein, we report a sprayable in situ forming hydrogel composed of poly(N-isopropylacrylamide166-co-n-butyl acrylate9)-poly(ethylene glycol)-poly(N-isopropylacrylamide166-co-n-butyl acrylate9) copolymer (P(NIPAM166-co-nBA9)-PEG-P(NIPAM166-co-nBA9), denoted as PEP) and silver-nanoparticles-decorated reduced graphene oxide nanosheets (Ag@rGO, denoted as AG) in response to skin temperature. This thermoresponsive hydrogel exhibits intriguing sol-gel irreversibility at low temperatures for the stable dressing of a wound, which is attributed to the inorganic/polymeric dual network and abundant coordination interactions between Ag@rGO nanosheets and PNIPAM. The biocompatibility and antibacterial ability against methicillin-resistant Staphylococcus aureus (MRSA) of this PEP-AG hydrogel wound dressing are confirmed in vitro and in vivo, which could transparently promote the healing of a MRSA-infected skin defect.

Keywords: hydrogel; in situ forming; irreversibility; methicillin-resistant Staphylococcus aureus; sol−gel transition; thermoresponsive; wound closure.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Acrylic Resins / chemical synthesis
  • Acrylic Resins / chemistry
  • Animals
  • Bandages
  • Biocompatible Materials / pharmacology
  • Graphite / chemistry
  • Hydrogels / chemical synthesis
  • Hydrogels / chemistry
  • Hydrogels / pharmacology*
  • Methicillin-Resistant Staphylococcus aureus / drug effects*
  • Microbial Sensitivity Tests
  • Oxidation-Reduction
  • Phase Transition*
  • Polyethylene Glycols / chemical synthesis
  • Polyethylene Glycols / chemistry
  • Rats, Sprague-Dawley
  • Skin / drug effects
  • Skin / microbiology
  • Skin / pathology
  • Temperature*
  • Wound Healing / drug effects*

Substances

  • Acrylic Resins
  • Biocompatible Materials
  • Hydrogels
  • graphene oxide
  • poly-N-isopropylacrylamide
  • Polyethylene Glycols
  • Graphite