Characterization of Fully Recombinant Human 20S and 20S-PA200 Proteasome Complexes

Mol Cell. 2019 Oct 3;76(1):138-147.e5. doi: 10.1016/j.molcel.2019.07.014. Epub 2019 Aug 28.

Abstract

Proteasomes are essential in all eukaryotic cells. However, their function and regulation remain considerably elusive, particularly those of less abundant variants. We demonstrate the human 20S proteasome recombinant assembly and confirmed the recombinant complex integrity biochemically and with a 2.6 Å resolution cryo-EM map. To assess its competence to form higher-order assemblies, we prepared and analyzed recombinant human 20S-PA200, a poorly characterized nuclear complex. Its 3.0 Å resolution cryo-EM structure reveals the PA200 unique architecture; the details of its intricate interactions with the proteasome, resulting in unparalleled proteasome α ring rearrangements; and the molecular basis for PA200 allosteric modulation of the proteasome active sites. Non-protein cryo-EM densities could be assigned to PA200-bound inositol phosphates, and we speculate regarding their functional role. Here we open extensive opportunities to study the fundamental properties of the diverse and distinct eukaryotic proteasome variants and to improve proteasome targeting under different therapeutic conditions.

Keywords: 20S-PA200; PA200; atomic model; cryo-EM; human; proteasome; recombinant; regulator; structure.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Allosteric Regulation
  • Animals
  • Binding Sites
  • Humans
  • Inositol Phosphates / metabolism
  • Models, Molecular
  • Nuclear Proteins / genetics
  • Nuclear Proteins / metabolism*
  • Nuclear Proteins / ultrastructure
  • Proteasome Endopeptidase Complex / genetics
  • Proteasome Endopeptidase Complex / metabolism*
  • Proteasome Endopeptidase Complex / ultrastructure
  • Protein Binding
  • Protein Conformation
  • Proteolysis
  • Recombinant Proteins / metabolism
  • Recombinant Proteins / ultrastructure
  • Sf9 Cells
  • Spodoptera
  • Structure-Activity Relationship

Substances

  • Inositol Phosphates
  • Nuclear Proteins
  • Recombinant Proteins
  • proteasome activator 200 kDa, human
  • Proteasome Endopeptidase Complex