Hyaluronic acid-coated pH sensitive poly (β-amino ester) nanoparticles for co-delivery of embelin and TRAIL plasmid for triple negative breast cancer treatment

Int J Pharm. 2020 Jan 5:573:118637. doi: 10.1016/j.ijpharm.2019.118637. Epub 2019 Sep 21.

Abstract

Triple negative breast cancer (TNBC) still lacks an effective targeted treatment. In this study, hyaluronic acid (HA)-mediated tumor targeting and pH-sensitive amphiphilic polymeric nanoparticles were designed and prepared to co-deliver the anticancer drug embelin (EMB) and tumor necrosis factor-related apoptosis-inducing ligand (TRAIL) plasmid (pTRAIL) (EMB/TRAIL-HA/PBAE-PEI) for synergistic anti-breast cancer efficacy. These pH-sensitive amphiphilic polymeric nanoparticles were formed using the amphiphilic polymers polyethyleneimine (PEI)-poly[(1,6-hexanediol)-diacrylate-β-5-hydroxyamylamine] (PBAE), which was synthesized via Michael addition polymerization. Taking advantage of the specific binding between HA and CD44, which is highly expressed in MDA-MB-231 TNBC cells, the HA-coated nanoparticles increased drug uptake in MDA-MB-231 TNBC cells compared with MCF-7 non-TNBC cells with lower CD44 expression. Moreover, EMB/TRAIL-HA/PBAE-PEI exhibited enhanced cytotoxic and pro-apoptotic effects against MDA-MB-231 cells compared with free EMB and EMB- or pTRAIL-loaded nanoparticles via activation of caspase 3/7, an increase in reactive oxygen species levels, and inhibition of the expressions of apoptosis-related proteins. These results demonstrated that EMB/TRAIL-HA/PBAE-PEI exerted enhanced cytotoxic and pro-apoptotic effects against MDA-MB-231 cells and showed great potential for TNBC treatment.

Keywords: Co-delivery; Embelin; Hyaluronic acid; Plasmid; pH-sensitive.

Publication types

  • Comparative Study

MeSH terms

  • Antineoplastic Agents / administration & dosage
  • Antineoplastic Agents / pharmacology
  • Apoptosis / drug effects
  • Benzoquinones / administration & dosage*
  • Benzoquinones / pharmacology
  • Cell Line, Tumor
  • Drug Carriers / chemistry
  • Female
  • Humans
  • Hyaluronan Receptors / metabolism
  • Hyaluronic Acid / chemistry
  • Hydrogen-Ion Concentration
  • MCF-7 Cells
  • Nanoparticles*
  • Plasmids
  • Polyethyleneimine / chemistry
  • Polymers / chemistry
  • Reactive Oxygen Species / metabolism
  • TNF-Related Apoptosis-Inducing Ligand / genetics*
  • Triple Negative Breast Neoplasms / pathology
  • Triple Negative Breast Neoplasms / therapy*

Substances

  • Antineoplastic Agents
  • Benzoquinones
  • CD44 protein, human
  • Drug Carriers
  • Hyaluronan Receptors
  • Polymers
  • Reactive Oxygen Species
  • TNF-Related Apoptosis-Inducing Ligand
  • poly(beta-amino ester)
  • Polyethyleneimine
  • Hyaluronic Acid
  • embelin