A Novel VIII Carboxylesterase with High Hydrolytic Activity Against Ampicillin from a Soil Metagenomic Library

Mol Biotechnol. 2019 Dec;61(12):892-904. doi: 10.1007/s12033-019-00220-3.

Abstract

A novel carboxylesterase gene, named dlfae4, was discovered and sequenced from a soil metagenomic library. The dlfae4 gene was composed of 1017 base pairs encoding 338 amino acid residues with a predicted molecular mass of 37.2 kDa. DLFae4 exhibited strong hydrolytic activity towards methyl ferulate under optimum pH and temperature conditions (pH 8.6, 50 °C) and displayed remarkable thermostability, with residual activity as high as 50% after incubation for 3 h at 60 °C. A family VIII esterase DLFae4 was found to contain a typical serine residue within the S-X-X-K motif, which serves as a catalytic nucleophile in class C β-lactamases and family VIII esterases. As a consequence of its high sequence similarity with β-lactamases, DLFae4 exhibited significant hydrolytic activity towards ampicillin. In addition, DLFae4 was found to be the first known member of family VIII carboxylesterases with phthalate-degrading ability. Site-directed mutagenesis studies revealed that Ser11, Lys14, and Tyr121 residues play an essential catalytic role in DLFae4. These new findings, which are of great importance for further in-depth research and engineering development of carboxylesterases, should advance the implementation of biotechnological applications.

Keywords: Carboxylesterase; Hydrolytic ampicillin; Metagenomics; Phthalate degradation; Thermostability.

MeSH terms

  • Amino Acid Sequence
  • Ampicillin / metabolism*
  • Carboxylesterase / chemistry*
  • Carboxylesterase / genetics*
  • Carboxylesterase / metabolism
  • Cloning, Molecular
  • Escherichia coli / genetics
  • Gene Expression
  • Gene Library
  • Hydrolysis
  • Kinetics
  • Metagenome*
  • Phthalic Acids / chemistry
  • Phylogeny
  • Sequence Alignment
  • Soil Microbiology
  • Substrate Specificity

Substances

  • Phthalic Acids
  • phthalic acid
  • Ampicillin
  • Carboxylesterase