Isolation and characterisation of GLP-1 7-36 amide from rat intestine. Elevated levels in diabetic rats

FEBS Lett. 1988 Dec 19;242(1):167-70. doi: 10.1016/0014-5793(88)81008-1.

Abstract

Glucagon-like peptide-1 (GLP-1) was purified to homogeneity by HPLC and anion-exchange chromatography. A molecular mass of 3297.4 Da was obtained by FAB mass spectrometry which corresponded exactly to GLP-1 7-36 NH2, providing evidence that amidation occurs at an arginine residue during the post-translational processing of GLP-1. The distribution of GLP-1 7-36 NH2-like immunoreactivity (GLP-1 7-36 NH2 IR) was determined in the rat gastrointestinal tract. Highest concentrations were found in terminal ileum and colon. Streptozocin-induced diabetic rats, who showed a significant increase in food intake, had a significant increase of GLP-1 7-36 NH2 IR in the colon.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Chromatography, High Pressure Liquid
  • Chromatography, Ion Exchange
  • Colon / analysis
  • Colon / metabolism
  • Diabetes Mellitus, Experimental / metabolism*
  • Eating
  • Glucagon
  • Glucagon-Like Peptide 1
  • Glucagon-Like Peptides
  • Ileum / analysis
  • Ileum / metabolism
  • Intestinal Mucosa / metabolism*
  • Intestines / analysis
  • Mass Spectrometry
  • Molecular Weight
  • Peptide Fragments*
  • Peptides / analysis
  • Peptides / isolation & purification
  • Peptides / metabolism*
  • Rats
  • Rats, Inbred Strains
  • Tissue Distribution

Substances

  • Peptide Fragments
  • Peptides
  • glucagon-like peptide 1 (7-36)amide
  • Glucagon-Like Peptides
  • Glucagon-Like Peptide 1
  • Glucagon