Affinity purification of tubulin from plant materials

Methods Cell Biol. 2020:160:263-280. doi: 10.1016/bs.mcb.2020.06.002. Epub 2020 Jul 22.

Abstract

In the plant cytoskeleton research, mammalian brain tubulin has been widely used to study plant microtubule-interacting proteins in vitro since purification of tubulins from plant sources is generally considered to be challenging and time-consuming. A convenient method for affinity purification of tubulins was devised, which utilized the TOG domains of yeast Stu2 tubulin-binding protein as an affinity ligand (Widlund et al., 2012). We showed that this so-called TOG tubulin affinity chromatography worked efficiently with plant materials, especially actively-dividing cultured cells (Hotta et al., 2016). Plant tubulins purified with the TOG method is highly assembly-competent and thus can be used in various in vitro experiments. Here, we summarize purification strategies of native or tagged plant tubulins as well as an in vitro pull-down assay to monitor their polymerization activity.

Keywords: Affinity purification; Microtubule; Posttranslational modifications; TOG; Tubulin; Tubulin mutation.

MeSH terms

  • Amino Acid Sequence
  • Arabidopsis / genetics
  • Arabidopsis / metabolism*
  • Chromatography, Affinity / methods*
  • Histidine / metabolism
  • Oligopeptides / metabolism
  • Plant Cells / metabolism
  • Plant Proteins / chemistry
  • Plant Proteins / isolation & purification*
  • Plants, Genetically Modified
  • Recombinant Fusion Proteins / metabolism
  • Tubulin / chemistry
  • Tubulin / isolation & purification*

Substances

  • His-His-His-His-His-His
  • Oligopeptides
  • Plant Proteins
  • Recombinant Fusion Proteins
  • Tubulin
  • Histidine