Benzyl and benzoyl benzoic acid inhibitors of bacterial RNA polymerase-sigma factor interaction

Eur J Med Chem. 2020 Dec 15:208:112671. doi: 10.1016/j.ejmech.2020.112671. Epub 2020 Aug 18.

Abstract

Transcription is an essential biological process in bacteria requiring a core enzyme, RNA polymerase (RNAP). Bacterial RNAP is catalytically active but requires sigma (σ) factors for transcription of natural DNA templates. σ factor binds to RNAP to form a holoenzyme which specifically recognizes a promoter, melts the DNA duplex, and commences RNA synthesis. Inhibiting the binding of σ to RNAP is expected to inhibit bacterial transcription and growth. We previously identified a triaryl hit compound that mimics σ at its major binding site of RNAP, thereby inhibiting the RNAP holoenzyme formation. In this study, we modified this scaffold to provide a series of benzyl and benzoyl benzoic acid derivatives possessing improved antimicrobial activity. A representative compound demonstrated excellent activity against Staphylococcus epidermidis with minimum inhibitory concentrations reduced to 0.5 μg/mL, matching that of vancomycin. The molecular mechanism of inhibition was confirmed using biochemical and cellular assays. Low cytotoxicity and metabolic stability of compounds demonstrated the potential for further studies.

Keywords: Antimicrobial; Bacterial transcription; Inhibitor; RNA polymerase; Sigma factor.

MeSH terms

  • Animals
  • Bacteria / drug effects
  • Bacterial Proteins / metabolism*
  • Benzoates / chemical synthesis
  • Benzoates / metabolism
  • Benzoates / pharmacology*
  • Benzophenones / chemical synthesis
  • Benzophenones / metabolism
  • Benzophenones / pharmacology*
  • Benzyl Compounds / chemical synthesis
  • Benzyl Compounds / metabolism
  • Benzyl Compounds / pharmacology*
  • DNA-Directed RNA Polymerases / metabolism*
  • Microbial Sensitivity Tests
  • Microsomes, Liver / metabolism
  • Protein Binding / drug effects
  • Rats
  • Sigma Factor / metabolism*

Substances

  • Bacterial Proteins
  • Benzoates
  • Benzophenones
  • Benzyl Compounds
  • Sigma Factor
  • DNA-Directed RNA Polymerases