Ex vivo assays to detect complement activation in complementopathies

Clin Immunol. 2020 Dec:221:108616. doi: 10.1016/j.clim.2020.108616. Epub 2020 Oct 24.

Abstract

In complement-driven thrombotic microangiopathies, failure to regulate complement activation leads to end-organ damage. The modified Ham (mHam) test measures complement-mediated killing of a nucleated cell in vitro but lacks a confirmatory assay and reliable positive controls. We demonstrate that C5b-9 accumulation on the surface of TF1 PIGAnull cells correlates with cell killing in the mHam. We also show that Sialidase treatment of cells or addition of Shiga toxin 1 to human serum serve as a more reliable positive control for the mHam than cobra venom factor or lipopolysaccharide. Simultaneously performing the mHam and measuring C5b-9 accumulation either in GVB++ or GVB0 MgEGTA buffer with the addition of complement pathway specific inhibitors (anti-C5 antibody or a factor D inhibitor, ACH-145951) can be used to localize defects in complement regulation. As more targeted complement inhibitors become available, these assays may aid in the selection of personalized treatments for patients with complement-mediated diseases.

Keywords: Atypical hemolytic uremic syndrome; Complement; Complement inhibitors; Modified HAM assay; Shiga toxin 1; Sialidase.

Publication types

  • Research Support, N.I.H., Extramural

MeSH terms

  • Adult
  • Antiphospholipid Syndrome / immunology*
  • Atypical Hemolytic Uremic Syndrome / immunology*
  • Biological Assay
  • Cell Line, Tumor
  • Complement Activation / drug effects*
  • Complement C3c / immunology
  • Complement C4b / immunology
  • Complement Inactivating Agents / pharmacology*
  • Complement Membrane Attack Complex / immunology
  • Elapid Venoms / pharmacology
  • Female
  • Humans
  • Lipopolysaccharides / pharmacology
  • Male
  • Middle Aged
  • Neuraminidase / pharmacology
  • Peptide Fragments / immunology
  • Shiga Toxin 1 / pharmacology

Substances

  • Complement Inactivating Agents
  • Complement Membrane Attack Complex
  • Elapid Venoms
  • Lipopolysaccharides
  • Peptide Fragments
  • Shiga Toxin 1
  • cobra venom factor
  • Complement C3c
  • Complement C4b
  • complement C4d
  • Neuraminidase