FGF23 contains two distinct high-affinity binding sites enabling bivalent interactions with α-Klotho

Proc Natl Acad Sci U S A. 2020 Dec 15;117(50):31800-31807. doi: 10.1073/pnas.2018554117. Epub 2020 Nov 30.

Abstract

The three members of the endocrine-fibroblast growth factor (FGF) family, FGF19, 21, and 23 are circulating hormones that regulate critical metabolic processes. FGF23 stimulates the assembly of a signaling complex composed of α-Klotho (KLA) and FGF receptor (FGFR) resulting in kinase activation, regulation of phosphate homeostasis, and vitamin D levels. Here we report that the C-terminal tail of FGF23, a region responsible for KLA binding, contains two tandem repeats, repeat 1 (R1) and repeat 2 (R2) that function as two distinct ligands for KLA. FGF23 variants with a single KLA binding site, FGF23-R1, FGF23-R2, or FGF23-wild type (WT) with both R1 and R2, bind to KLA with similar binding affinity and stimulate FGFR1 activation and MAPK response. R2 is flanked by two cysteines that form a disulfide bridge in FGF23-WT; disulfide bridge formation in FGF23-WT is dispensable for KLA binding and for cell signaling via FGFRs. We show that FGF23-WT stimulates dimerization and activation of a chimeric receptor molecule composed of the extracellular domain of KLA fused to the cytoplasmic domain of FGFR and employ total internal reflection fluorescence microscopy to visualize individual KLA molecules on the cell surface. These experiments demonstrate that FGF23-WT can act as a bivalent ligand of KLA in the cell membrane. Finally, an engineered Fc-R2 protein acts as an FGF23 antagonist offering new pharmacological intervention for treating diseases caused by excessive FGF23 abundance or activity.

Keywords: biological inhibitor; cell signaling; endocrine FGF; phosphorylation; surface receptors.

MeSH terms

  • Binding Sites
  • Calcinosis / drug therapy
  • Calcinosis / genetics
  • Cell Membrane / metabolism
  • Fibroblast Growth Factor-23
  • Fibroblast Growth Factors / genetics
  • Fibroblast Growth Factors / metabolism*
  • Fibroblast Growth Factors / therapeutic use
  • Glucuronidase / metabolism*
  • HEK293 Cells
  • Humans
  • Hyperostosis, Cortical, Congenital / drug therapy
  • Hyperostosis, Cortical, Congenital / genetics
  • Hyperphosphatemia / drug therapy
  • Hyperphosphatemia / genetics
  • Immunoglobulin Fc Fragments / genetics
  • Immunoglobulin Fc Fragments / therapeutic use
  • Klotho Proteins
  • Mutation
  • Osteomalacia / drug therapy
  • Osteomalacia / genetics
  • Protein Binding / drug effects
  • Protein Binding / physiology
  • Protein Domains
  • Protein Multimerization / drug effects
  • Protein Multimerization / physiology*
  • Recombinant Fusion Proteins / genetics
  • Recombinant Fusion Proteins / therapeutic use
  • Rickets, Hypophosphatemic / drug therapy
  • Rickets, Hypophosphatemic / genetics

Substances

  • FGF23 protein, human
  • Immunoglobulin Fc Fragments
  • Recombinant Fusion Proteins
  • Fibroblast Growth Factors
  • Fibroblast Growth Factor-23
  • Glucuronidase
  • Klotho Proteins

Supplementary concepts

  • Tumoral Calcinosis, Hyperphosphatemic, Familial