Covalent Linkage of BODIPY-Photosensitizers to Anderson-Type Polyoxometalates Using CLICK Chemistry

Chemistry. 2021 Dec 6;27(68):17181-17187. doi: 10.1002/chem.202102897. Epub 2021 Sep 29.

Abstract

The covalent attachment of molecular photosensitizers (PS) to polyoxometalates (POMs) opens new pathways to PS-POM dyads for light-driven charge-transfer and charge-storage. Here, we report a synthetic route for the covalent linkage of BODIPY-dyes to Anderson-type polyoxomolybdates by using CLICK chemistry (i. e. copper-catalyzed azide-alkyne cycloaddition, CuAAC). Photophysical properties of the dyad were investigated by combined experimental and theoretical methods and highlight the role of both sub-components for the charge-separation properties. The study demonstrates how CLICK chemistry can be used for the versatile linkage of organic functional units to molecular metal oxide clusters.

Keywords: BODIPY; organo-functionalization; photophysics; polyoxometalates; self-assembly.

MeSH terms

  • Anions
  • Azides
  • Boron Compounds
  • Click Chemistry*
  • Photosensitizing Agents*
  • Polyelectrolytes

Substances

  • 4,4-difluoro-4-bora-3a,4a-diaza-s-indacene
  • Anions
  • Azides
  • Boron Compounds
  • Photosensitizing Agents
  • Polyelectrolytes
  • polyoxometalate