Total Syntheses of Proposed Structures of 4,10-Dihydroxy-8,12-guaianolides

Org Lett. 2022 May 6;24(17):3297-3301. doi: 10.1021/acs.orglett.2c01215. Epub 2022 Apr 21.

Abstract

The first total syntheses of two 4,10-dihydroxy-8,12-guaianolides that were reported to be natural products were achieved. Toward the syntheses of a collection of related guaianolides, the typical 5,7-fused system of 8,12-guaianolides was constructed by a ring expansion reaction of a hydroxylated coronafacic acid analogue that can be practically synthesized and optically resolved. The total syntheses of these compounds revealed that the previously reported structures of both natural products were incorrect.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Biological Products* / chemistry
  • Molecular Structure

Substances

  • Biological Products