Delayed light activation of resin composite affects the bond strength of adhesives under dynamic simulated pulpal pressure

Clin Oral Investig. 2022 Nov;26(11):6743-6752. doi: 10.1007/s00784-022-04634-3. Epub 2022 Jul 25.

Abstract

Objective: To evaluate the effect of a time delay before the light activation of resin composite on the microtensile bond strength (µTBS) of self-etch adhesives under dynamic simulated pulpal pressure.

Materials and methods: One hundred twenty crown segments were prepared from human third molars. Dentin surfaces were prepared with coarse diamond burs and connected to a dynamic pulpal pressure device. The self-etch adhesives used were Clearfil SE Bond (CSE), G2-Bond Universal (G2B), Clearfil Universal Bond Quick (CBQ), and G-Premio Bond (GPB). Each adhesive was divided into 3 subgroups: immediate light activation of resin composite (T0), delayed light activation for 150 s (T1), and 300 s (T2). The µTBS data were obtained after 24-h water storage. Scanning electron microscopy was used to evaluate the nanoleakage at the resin-dentin surface. The µTBS data were analyzed using two-way ANOVA and Duncan's multiple comparisons.

Results: All adhesives demonstrated a significant reduction in µTBS at T2, except for CBQ where the bond strength was not affected by the delayed light activation times. The two-step self-etch adhesives (CSE and G2B) demonstrated higher bond strength than the one-step adhesives at all conditions. Nanoleakage was observed in all adhesives at T2; however, nanoleakage was detected only in CBQ and GPB at T1.

Conclusions: Delayed light activation of resin composite adversely affected the dentin bond strength of self-etch adhesives. Two-step self-etch adhesives had better bonding performance than one-step self-etch adhesives.

Clinical relevance: After adhesive application, resin composite should be adapted and cured as soon as possible.

Keywords: Dynamic simulated pulpal pressure; Light activation; Microtensile bond strength; Nanoleakage; Self-etch adhesive.

MeSH terms

  • Adhesives
  • Composite Resins / chemistry
  • Dental Bonding*
  • Dental Cements
  • Dentin
  • Dentin-Bonding Agents / chemistry
  • Humans
  • Materials Testing
  • Resin Cements / chemistry
  • Tensile Strength

Substances

  • Dental Cements
  • Bis-GMA, BPDM, HEMA dental-bonding resin
  • Dentin-Bonding Agents
  • Resin Cements
  • Composite Resins
  • G-Bond
  • Adhesives