Identification and characterization of a novel thermo-stable endo-β-N-acetylglucosaminidase from Rhizomucorpusillus

J Biosci Bioeng. 2022 Oct;134(4):295-300. doi: 10.1016/j.jbiosc.2022.06.013. Epub 2022 Aug 10.

Abstract

Endo-β-N-acetylglucosaminidase (ENGase) is an enzyme that hydrolyzes the chitobiose core of N-glycans and is widely used for glycan analysis on glycoproteins and preparation of precursors for glycosylated compounds. While most of the ENGases that can hydrolyze complex-type glycans are derived from eukaryotes, their production by heterologous expression using Escherichia coli is insufficient, making the production process expensive. From an industrial perspective, there is a need for a less expensive enzyme with higher activity and stability. In this study, we identified a novel ENGase gene from a thermophilic fungus, Rhizomucor pusillus, and named it Endo-Rp. Characterization of the recombinant Endo-Rp showed that the enzyme had maximum hydrolytic activity at 60 °C and hydrolyzed high-mannose-type and biantennary complex-type glycans, but not (2,4)-branched triantennary complex-type or fucosylated glycans. Endo-Rp also hydrolyzed N-glycans attached to RNase B and human transferrin. In summary, we consider Endo-Rp to be a valuable enzyme in various scientific and industrial applications.

Keywords: Endo-β-N-acetylglucosaminidase; Endoglycosidase; Glycoside hydrolase family 85; N-glycan; Rhizomucor pusillus.

MeSH terms

  • Acetylglucosaminidase* / genetics
  • Acetylglucosaminidase* / metabolism
  • Glycoproteins / metabolism
  • Humans
  • Mannose* / metabolism
  • Mannosyl-Glycoprotein Endo-beta-N-Acetylglucosaminidase / genetics
  • Mannosyl-Glycoprotein Endo-beta-N-Acetylglucosaminidase / metabolism
  • Polysaccharides / genetics
  • Polysaccharides / metabolism
  • Transferrins

Substances

  • Glycoproteins
  • Polysaccharides
  • Transferrins
  • Acetylglucosaminidase
  • Mannosyl-Glycoprotein Endo-beta-N-Acetylglucosaminidase
  • Mannose