Optical properties, biaxial flexural strength, and reliability of new-generation lithium disilicate glass-ceramics after thermal cycling

Purpose: To investigate the color stability, translucency, biaxial flexural strength (BFS), and reliability of nano-lithium disilicate and fully crystallized lithium disilicate after thermal cycling and to compare with those of a commonly used lithium disilicate.

Materials and methods: Three lithium disilicate glass-ceramics were used to prepare disk-shaped specimens (ø:12 mm, thickness: 1.2 mm) from A2 shaded HT blocks (Amber Mill, AM; Initial LiSi Block, IN; IPS e.max CAD, EX). AM and EX specimens were crystallized, and all specimens were polished with a polishing paste (Diamond Polish Mint). A spectrophotometer (CM-26d) was used to measure color coordinates before and after thermal cycling. BFS test was performed after thermal cycling. Color differences (ΔE₀₀ ) and relative translucency parameter (RTP) values were calculated. One-way analysis of variance (ANOVA) (ΔE₀₀ and BFS), two-way ANOVA followed by Tukey's HSD tests (RTP), and chi-square tests (Weibull modulus and characteristic strength) were used for the statistical analyses (α = 0.05).

Results: No significant differences were observed among the ΔE₀₀ values of tested materials (df = 2, F = 2.933, p = 0.070). RTP values were only affected by material type (p < 0.001) as AM had the highest RTP (p < 0.001), whereas IN and EX had similar values (p ≥ 0.165). BFS values varied among tested materials (df = 2, F = 21.341, p < 0.001). AM and EX had similar BFS values (p = 0.067) that were higher than that of IN (p ≤ 0.001). Weibull moduli of the materials were similar (p = 0.305), whereas EX had the highest and IN had the lowest characteristic strength values (p < 0.001) CONCLUSIONS: Although nano-lithium disilicate had the highest translucency, all materials had imperceptible color and translucency changes after thermal cycling when reported threshold values were considered. Newly introduced lithium disilicate glass-ceramics had adequate flexural strength as compared to the precursor material.