Graphene sandwich-based biological specimen preparation for cryo-EM analysis

Proc Natl Acad Sci U S A. 2024 Jan 30;121(5):e2309384121. doi: 10.1073/pnas.2309384121. Epub 2024 Jan 22.

Abstract

High-quality specimen preparation plays a crucial role in cryo-electron microscopy (cryo-EM) structural analysis. In this study, we have developed a reliable and convenient technique called the graphene sandwich method for preparing cryo-EM specimens. This method involves using two layers of graphene films that enclose macromolecules on both sides, allowing for an appropriate ice thickness for cryo-EM analysis. The graphene sandwich helps to mitigate beam-induced charging effect and reduce particle motion compared to specimens prepared using the traditional method with graphene support on only one side, therefore improving the cryo-EM data quality. These advancements may open new opportunities to expand the use of graphene in the field of biological electron microscopy.

Keywords: beam-induced motion; charging effect; cryo-EM; graphene sandwich; sample preparation.

MeSH terms

  • Cryoelectron Microscopy
  • Data Accuracy
  • Graphite*
  • Motion

Substances

  • Graphite