Pseudodiproline (Pro-Cyp) Oligomers Fold into Helical Polyproline Type secondary structures

J Org Chem. 2024 Apr 5;89(7):4283-4293. doi: 10.1021/acs.joc.3c02840. Epub 2024 Mar 15.

Abstract

The synthesis and conformational properties of oligo-proline mimetics composed of dimeric and tetrameric Pro-Cyp constructs linked by a hydroxymethylene unit are reported. Oligomers were studied both in the solid state and in solution, unveiling right-handed helical conformation depending on the configuration of the vicinally substituted trans-cyclopentane carboxylic acid unit (Cyp). Unlike polyproline oligomers, the alternating synthetic Pro-Cyp counterparts are not stabilized by n-π* interactions but rely instead on the steric demands of the extended backbone conformation within the hydroxymethylene-linked Pro-Cyp repeating units.

Publication types

  • Review