Aqueous biphasic systems developed with deep eutectic solvents and polymer for the efficient extraction of pigments from beverages

Food Chem. 2024 Aug 15:449:139206. doi: 10.1016/j.foodchem.2024.139206. Epub 2024 Mar 31.

Abstract

Novel aqueous biphasic systems (ABSs) developed with benzyl-based quaternary ammonium salts-deep eutectic solvents (DESs) and polypropylene glycol (PPG) were herein proposed. The liquid-liquid equilibrium and the partitioning behavior of pigments in the systems were addressed. The results suggested that the shorter the carbon chain length of the DES, the easier to form two phases. The analysis of mixed samples showed that the selective separation was achieved in the ABSs, including 99.47% of tartrazine in the DES-rich phase and 98.47% of sudan III in the PPG-rich phase. Additionally, the systems were successfully applied to the extraction of pigments from the actual beverage samples with recoveries ranging from 93.43% to 102.15%. Furthermore, the study on the separation mechanism indicated that the hydrogen bonding played a significant role in the separation process. All the above results highlight the proposed DES/polymer-based ABSs have great advantages in selective and high-performance separation of pigments from beverages.

Keywords: Aqueous biphasic systems; Deep eutectic solvent; Extraction; Pigment; Polymer.

Publication types

  • Evaluation Study

MeSH terms

  • Azo Compounds*
  • Beverages* / analysis
  • Coloring Agents / chemistry
  • Coloring Agents / isolation & purification
  • Deep Eutectic Solvents* / chemistry
  • Polymers* / chemistry
  • Propylene Glycols / chemistry
  • Propylene Glycols / isolation & purification
  • Quaternary Ammonium Compounds / chemistry
  • Solvents / chemistry

Substances

  • Polymers
  • Deep Eutectic Solvents
  • polypropylene glycol
  • Propylene Glycols
  • Coloring Agents
  • Solvents
  • Quaternary Ammonium Compounds
  • sudan III
  • Azo Compounds