Curved Nanographenes as Stoppers in a [2]Rotaxane with Two-Photon Excited Emission

J Org Chem. 2024 Jul 5;89(13):9344-9351. doi: 10.1021/acs.joc.4c00486. Epub 2024 Jun 22.

Abstract

Heptagon-containing distorted nanographenes are used as stoppers for the capping of a [2]rotaxane through a Michael-type addition reaction to vinyl sulfone groups. These curved aromatics are bulky enough to prevent the disassembly of the rotaxane but also give emissive and nonlinear (two-photon absorption and emission) optical properties to the structure.