Therapeutic impacts of GNE‑477‑loaded H2O2 stimulus‑responsive dodecanoic acid‑phenylborate ester‑dextran polymeric micelles on osteosarcoma

Int J Mol Med. 2024 Aug;54(2):69. doi: 10.3892/ijmm.2024.5393. Epub 2024 Jun 28.

Abstract

Osteosarcoma (OS) is a highly malignant primary bone neoplasm that is the leading cause of cancer‑associated death in young people. GNE‑477 belongs to the second generation of mTOR inhibitors and possesses promising potential in the treatment of OS but dose tolerance and drug toxicity limit its development and utilization. The present study aimed to prepare a novel H2O2 stimulus‑responsive dodecanoic acid (DA)‑phenylborate ester‑dextran (DA‑B‑DEX) polymeric micelle delivery system for GNE‑477 and evaluate its efficacy. The polymer micelles were characterized by morphology, size and critical micelle concentration. The GNE‑477 loaded DA‑B‑DEX (GNE‑477@DBD) tumor‑targeting drug delivery system was established and the release of GNE‑477 was measured. The cellular uptake of GNE‑477@DBD by three OS cell lines (MG‑63, U2OS and 143B cells) was analyzed utilizing a fluorescent tracer technique. The hydroxylated DA‑B was successfully grafted onto dextran at a grafting rate of 3%, suitable for forming amphiphilic micelles. Following exposure to H2O2, the DA‑B‑DEX micelles ruptured and released the drug rapidly, leading to increased uptake of GNE‑477@DBD by cells with sustained release of GNE‑477. The in vitro experiments, including MTT assay, flow cytometry, western blotting and RT‑qPCR, demonstrated that GNE‑477@DBD inhibited tumor cell viability, arrested cell cycle in G1 phase, induced apoptosis and blocked the PI3K/Akt/mTOR cascade response. In vivo, through the observation of mice tumor growth and the results of H&E staining, the GNE‑477@DBD group exhibited more positive therapeutic outcomes than the free drug group with almost no adverse effects on other organs. In conclusion, H2O2‑responsive DA‑B‑DEX presents a promising delivery system for hydrophobic anti‑tumor drugs for OS therapy.

Keywords: GNE‑477; PI3K/Akt/mTOR cascade response; osteosarcoma; polymeric micelles; stimulus‑responsive.

MeSH terms

  • Animals
  • Antineoplastic Agents / chemistry
  • Antineoplastic Agents / pharmacology
  • Apoptosis / drug effects
  • Bone Neoplasms / drug therapy
  • Bone Neoplasms / pathology
  • Cell Line, Tumor
  • Dextrans* / chemistry
  • Humans
  • Hydrogen Peroxide*
  • Lauric Acids* / chemistry
  • Lauric Acids* / pharmacology
  • Male
  • Mice
  • Mice, Inbred BALB C
  • Mice, Nude
  • Micelles*
  • Osteosarcoma* / drug therapy
  • Osteosarcoma* / pathology
  • Polymers / chemistry
  • Polymers / pharmacology
  • TOR Serine-Threonine Kinases / metabolism
  • Xenograft Model Antitumor Assays

Substances

  • Micelles
  • Hydrogen Peroxide
  • Dextrans
  • Lauric Acids
  • lauric acid
  • Polymers
  • Antineoplastic Agents
  • TOR Serine-Threonine Kinases

Grants and funding

The present study was supported by Department of Education of Guangxi Zhuang Autonomous Region, Project of Enhancing the Basic Research Ability of Young Teachers in Colleges and Universities (grant no. 2021KY0105) and Nanning First People's Hospital Scientific Research and Technology Development Program Project (grant no. 2021001).