Covalent post-synthetic modification of MOFs as a fluorescent sensor for the efficient detection of the biomarker of cystinuria

Mikrochim Acta. 2024 Jun 29;191(7):432. doi: 10.1007/s00604-024-06519-6.

Abstract

Cystinuria is a genetic disorder, and in severe cases, it might lead to kidney failure. As an important biomarker for cystinuria, the level of arginine (Arg) in urine is a vital indicator for cystinuria screening. Therefore, it is urgently needed to detect Arg with high selectivity and sensitivity. In this work, a boric acid functionalized Zr-based metal-organic framework UiO-PhbA is prepared by grafting phenylboronic acid on UiO-66-NH2 through a Schiff base reaction using a covalent post-synthesis modification (CPSM) strategy. The prepared UiO-PhbA exhibits a sensitive and specific fluorescence "turn-on" response to Arg and can be exploited to detect Arg in human serum and urine samples with a broad linear range of 0.6-350 µM and low limit of detection (LOD) of 18.45 nM. This study provides a new and reliable rapid screening protocol for sulfite oxidase deficiency-related diseases.

Keywords: Arginine; Biomarker; Covalent post-synthetic modification; Cystinuria; Fluorescence; Metal–organic frameworks.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Arginine* / blood
  • Arginine* / chemistry
  • Biomarkers* / blood
  • Biomarkers* / urine
  • Boronic Acids* / chemistry
  • Cystinuria* / diagnosis
  • Cystinuria* / urine
  • Fluorescent Dyes* / chemistry
  • Humans
  • Limit of Detection*
  • Metal-Organic Frameworks* / chemistry
  • Spectrometry, Fluorescence / methods
  • Zirconium / chemistry

Substances

  • Metal-Organic Frameworks
  • Fluorescent Dyes
  • Arginine
  • Biomarkers
  • Boronic Acids
  • Zirconium
  • benzeneboronic acid