[Validation of a method for measuring the antielastolytic activity of human circulating alpha1-antitrypsin]

Ann Biol Clin (Paris). 2024 Aug 30;82(3):308-320. doi: 10.1684/abc.2024.1893.
[Article in French]

Abstract

The existence of alpha-1 antitrypsin variants with apparently unremarkable phenotypes and serum concentrations, contrasting with a clinical picture suggestive of a severe deficiency, led us to investigate whether in these cases there was a reduction or even suppression of the capacity of alpha-1 antitrypsin to inhibit elastase. To this end, in two different laboratories, we adapted and validated a method for measuring the functional activity of alpha-1 antitrypsin, based on spectrophotometric kinetic analysis of the inhibition by serum alpha-1 antitrypsin of the hydrolytic activity of porcine pancreatic elastase on a chromogenic substrate. This method has proved to be robust, reproducible and transferable and made possible to define, on the basis of an analysis of a hospital population, a functionality index with a confidence interval comprised between 0.87 and 1.2, allowing to identify subjects likely to have a functional deficiency of alpha-1 antitrypsin, whether this deficiency being of a genetic origin without any quantitative or phenotypic translation, or whether being acquired under the effect of external agents (cigarette smoke or viruses).

Keywords: alpha1-antitrypsin deficiency; elastase-inhibitory capacity; method validation.

Publication types

  • Validation Study
  • English Abstract

MeSH terms

  • Adult
  • Animals
  • Female
  • Humans
  • Male
  • Middle Aged
  • Pancreatic Elastase* / analysis
  • Pancreatic Elastase* / blood
  • Reproducibility of Results
  • Spectrophotometry / methods
  • Swine
  • alpha 1-Antitrypsin Deficiency* / blood
  • alpha 1-Antitrypsin Deficiency* / diagnosis
  • alpha 1-Antitrypsin* / analysis
  • alpha 1-Antitrypsin* / blood

Substances

  • alpha 1-Antitrypsin
  • Pancreatic Elastase