Azobenzene-based liposomes with nanomechanical action for cytosolic chemotherapeutic drug delivery

Colloids Surf B Biointerfaces. 2025 Jan:245:114198. doi: 10.1016/j.colsurfb.2024.114198. Epub 2024 Aug 31.

Abstract

The stimuli-responsive nano-carriers are at the forefront of research in nanotechnology and materials science. These advanced systems are designed to alter their physicochemical properties upon exposure to specific stimuli, enabling controllable and targeted delivery of therapeutic agents. Nevertheless, limited endosomal escape reduces the drug bioavailability in clinical use. We herein report azobenzene (Azo)-based liposomes, prepared by co-assembling the photoisomerizable cationic Azo lipids and helper lipids, which achieve controllable doxorubicin (Dox) release and enhanced cytosolic transport upon light irradiation. Azo lipids undergo reversible isomerization between cis-isomers and trans-isomer when received UV and visible (Vis) light irradiation, causing liposomal membrane permeability changes for controlled drug release. Moreover, the nanomechanical action created by the isomerization of Azo lipids promotes the endosomal escape of the liposomes. DSPC-Azo liposomes, with minimal Dox leakage, showed significant tumor cell killing upon irradiation. For in vivo study, we co-encapsulated the upconverting nanoparticles (UCNPs), which can convert the near-infrared (NIR) light into UV/Vis emissions, facilitating Azo units activation. UCNP/Dox-loaded DSPC-Azo liposomes inhibited tumor growth under NIR irradiation in a 4T1 tumor-bearing mouse model.

Keywords: Azobenzene-based liposome; Controllable drug release; Endosomal escape; Nanomechanical action; Photoisomerization.

MeSH terms

  • Animals
  • Antibiotics, Antineoplastic / administration & dosage
  • Antibiotics, Antineoplastic / chemistry
  • Antibiotics, Antineoplastic / pharmacology
  • Antineoplastic Agents / administration & dosage
  • Antineoplastic Agents / chemistry
  • Antineoplastic Agents / pharmacology
  • Azo Compounds* / chemistry
  • Azo Compounds* / pharmacology
  • Cell Line, Tumor
  • Cell Proliferation / drug effects
  • Cell Survival / drug effects
  • Cytosol / metabolism
  • Doxorubicin* / administration & dosage
  • Doxorubicin* / chemistry
  • Doxorubicin* / pharmacology
  • Drug Delivery Systems*
  • Drug Liberation
  • Drug Screening Assays, Antitumor
  • Female
  • Humans
  • Liposomes* / chemistry
  • Mice
  • Mice, Inbred BALB C
  • Nanoparticles / chemistry
  • Particle Size

Substances

  • Azo Compounds
  • azobenzene
  • Liposomes
  • Doxorubicin
  • Antineoplastic Agents
  • Antibiotics, Antineoplastic