Azamollugin, a mollugin derivative, has inhibitory activity on MyD88- and TRIF-dependent pathways

J Nat Med. 2025 Jan;79(1):36-44. doi: 10.1007/s11418-024-01842-x. Epub 2024 Sep 16.

Abstract

Previously, we reported that azamollugin, an aza-derivative of mollugin, exhibited potent inhibitory activity on NO production in LPS-stimulated RAW 264.7 cells. Further investigations in this study revealed that azamollugin not only suppressed iNOS gene expression regulated by NF-κB, but also inhibited LPS-induced IFN-β expression, which is known to be regulated by IRF3. Azamollugin exhibited an inhibitory activity on LPS-induced IRAK1 activation, suggesting inhibitory effect on the MyD88-dependent pathway. Furthermore, azamollugin inhibited LPS-induced phosphorylation of IRF3 and its upstream factor, TBK1/IKKε, suggesting an inhibitory effect on the TRIF-dependent pathway via TLR4. In addition, azamollugin also suppressed poly(I:C)-induced phosphorylation of TBK1 and IRF3, suggesting an inhibitory effect on the TRIF-dependent pathway via TLR3. These results suggest that azamollugin has inhibitory activity against both the MyD88-dependent and TRIF-dependent pathways, respectively.

Keywords: Anti-inflammatory; Azamollugin; IFN-β; IKKε; IRAK1; IRF3; Mollugin; NF-κB; Oxomollugin; TBK1.

MeSH terms

  • Adaptor Proteins, Vesicular Transport* / metabolism
  • Animals
  • Interferon Regulatory Factor-3 / metabolism
  • Interferon-beta / metabolism
  • Lipopolysaccharides / pharmacology
  • Mice
  • Myeloid Differentiation Factor 88* / metabolism
  • NF-kappa B / antagonists & inhibitors
  • NF-kappa B / metabolism
  • Nitric Oxide Synthase Type II / antagonists & inhibitors
  • Nitric Oxide Synthase Type II / metabolism
  • Phosphorylation / drug effects
  • Protein Serine-Threonine Kinases / antagonists & inhibitors
  • Protein Serine-Threonine Kinases / metabolism
  • RAW 264.7 Cells
  • Signal Transduction* / drug effects
  • Toll-Like Receptor 4 / metabolism

Substances

  • Myeloid Differentiation Factor 88
  • Adaptor Proteins, Vesicular Transport
  • TICAM-1 protein, mouse
  • Interferon Regulatory Factor-3
  • Myd88 protein, mouse
  • Tbk1 protein, mouse
  • Lipopolysaccharides
  • Protein Serine-Threonine Kinases
  • NF-kappa B
  • Nitric Oxide Synthase Type II
  • Interferon-beta
  • Irf3 protein, mouse
  • Toll-Like Receptor 4