Copper-based metal-organic framework co-loaded doxorubicin and curcumin for anti-cancer with synergistic apoptosis and ferroptosis therapy

Int J Pharm. 2024 Dec 5:666:124744. doi: 10.1016/j.ijpharm.2024.124744. Epub 2024 Sep 22.

Abstract

The combination of chemotherapy and ferroptosis therapy can greatly improve the efficiency of tumor treatment. However, ferroptosis-based therapy is limited by the unsatisfactory Fenton activity and insufficient H2O2 supply in tumor cells. In this work, a nano-drug delivery system Cur@DOX@MOF-199 NPs was constructed to combine ferroptosis and apoptosis by loading curcumin (Cur) and doxorubicin (DOX) based on the copper-based organic framework MOF-199. Cur@DOX@MOF-199 NPs decompose quickly by glutathione (GSH), releasing Cu2+, DOX and Cur. Cu2+ can deplete GSH while also being reduced to Cu+; DOX can induce apoptosis and simultaneously boost H2O2 production. Moreover, Cur enhanced the expression of intracellular heme oxygenase-1 (HO-1), for decomposing heme and releasing Fe2+, which further combined with Cu+ to catalyze H2O2 for hydroxyl radical (OH) generation, leading to the accumulation of lipid peroxide and ferroptosis. As a result, Cur@DOX@MOF-199 NPs exhibited significantly enhanced antitumor efficacy in MCF-7 tumor-bearing mouse model, suggesting this nano formulation is an excellent synergetic pathway for apoptosis and ferroptosis.

Keywords: Chemotherapy; Curcumin; Ferroptosis; Heme oxygenase 1; Metal-organic framework.

MeSH terms

  • Animals
  • Antineoplastic Agents / administration & dosage
  • Antineoplastic Agents / chemistry
  • Antineoplastic Agents / pharmacology
  • Apoptosis* / drug effects
  • Copper* / administration & dosage
  • Copper* / chemistry
  • Curcumin* / administration & dosage
  • Curcumin* / chemistry
  • Curcumin* / pharmacology
  • Doxorubicin* / administration & dosage
  • Doxorubicin* / chemistry
  • Doxorubicin* / pharmacology
  • Drug Synergism
  • Female
  • Ferroptosis* / drug effects
  • Glutathione / metabolism
  • Humans
  • Hydrogen Peroxide
  • MCF-7 Cells
  • Metal-Organic Frameworks* / chemistry
  • Mice
  • Mice, Inbred BALB C
  • Mice, Nude
  • Nanoparticle Drug Delivery System / chemistry
  • Nanoparticles / chemistry
  • Xenograft Model Antitumor Assays

Substances

  • Curcumin
  • Doxorubicin
  • Metal-Organic Frameworks
  • Copper
  • Antineoplastic Agents
  • Hydrogen Peroxide
  • Glutathione
  • Nanoparticle Drug Delivery System