Gypenoside A-loaded mPEG-PLGA nanoparticles ameliorate high-glucose-induced retinal microvasculopathy by inhibiting ferroptosis

Int J Pharm. 2024 Dec 5:666:124758. doi: 10.1016/j.ijpharm.2024.124758. Epub 2024 Sep 24.

Abstract

Diabetic retinopathy (DR) is one of the chronic microvascular complications of type 2 diabetes mellitus (T2DM), which will cause retinal detachment and blindness without ideal therapies. Gypenoside A (GPA) are the main bioactive compound from Gynostemma pentaphyllum, and have various pharmacological effects. However, it suffered from poor bioavailability and potential cardiotoxicity in the clinical application. To overcome those limitations, in this study, nearly spherical nanoparticles (GPA-NP) with a mean particle size of 140.6 ± 22.4 nm were prepared by encapsulating GPA into mPEG-PLGA. This encapsulation efficiency was 84.4 ± 6.9 %, and the drug load was 4.02 %±0.35 %. The results showed that GPA-NP displayed more prolonged GPA release and higher bioavailability in vitro than GPA. GPA-NP obviously reduced the levels of oxidative stress markers and inflammatory cytokines in both retinal tissues of DR mice and high glucose-exposed HRMEC better than GPA alone. Mechanismly, GPA blocked the Nrf2-Keap1 interaction by binding with Kelch domain of Keap1 via alkyl and hydrogen bonds. Therefore, GPA-NP exerted more potent protectivity effects against high glucose-induced retinal microvascular endothelial ferroptosis in vitro and in vivo by activating Nrf2/HO-1/GPX4 pathway. It could be a promising therapeutic agent for preventing DR.

Keywords: Ferroptosis; Keap1 inhibition; Oxidative stress.

MeSH terms

  • Animals
  • Cell Line
  • Diabetic Retinopathy* / drug therapy
  • Drug Carriers / chemistry
  • Drug Liberation
  • Endothelial Cells / drug effects
  • Endothelial Cells / metabolism
  • Ferroptosis* / drug effects
  • Glucose* / metabolism
  • Gynostemma* / chemistry
  • Humans
  • Kelch-Like ECH-Associated Protein 1 / metabolism
  • Male
  • Mice
  • Mice, Inbred C57BL
  • NF-E2-Related Factor 2 / metabolism
  • Nanoparticles*
  • Oxidative Stress / drug effects
  • Particle Size
  • Plant Extracts
  • Polyesters
  • Polyethylene Glycols* / chemistry
  • Retina / drug effects
  • Retina / metabolism

Substances

  • Polyethylene Glycols
  • gypenoside
  • methoxypolyethyleneglycol-poly(lactic-co-glycolic acid)
  • Glucose
  • NF-E2-Related Factor 2
  • Drug Carriers
  • Kelch-Like ECH-Associated Protein 1
  • Nfe2l2 protein, mouse
  • Plant Extracts
  • Polyesters