Flurbiprofen inhibits cAMP transport by MRP4/ABCC4 increasing the potency of gemcitabine treatment in PDAC cell models

Int J Biol Macromol. 2024 Nov;280(Pt 4):136386. doi: 10.1016/j.ijbiomac.2024.136386. Epub 2024 Oct 6.

Abstract

Pancreatic ductal adenocarcinoma (PDAC) remains a highly malignant cancer with a grim prognosis due to its early metastasis and resistance to current chemotherapies, such as Gemcitabine (GEM). We have previously demonstrated that cAMP exclusion by MRP4 is critical for PDAC cell proliferation, establishing this transporter as a promising prognostic marker and therapeutic target. In search for novel therapeutic options to improve GEM efficacy, we conducted a drug repositioning screening to identify potential inhibitors of cAMP transport by MRP4. Several non-steroidal anti-inflammatory drugs (NSAIDs) can inhibit the transport of certain MRP4 substrates. In this study, we assessed the efficacy of sixteen NSAIDs in inhibiting cAMP transport mediated by MRP4, identifying seven potent inhibitors based on their IC50 values. The most potent inhibitors were further tested for their effect on cell proliferation and migration. Flurbiprofen emerged as the most potent inhibitor of both MRP4-mediated cAMP transport and cell proliferation. Overexpression of MRP4 in BxPC-3 cells significantly increased GEM resistance, and co-administration of flurbiprofen with GEM markedly enhanced the latter's potency inhibiting PDAC cells proliferation. These findings position flurbiprofen as a potent inhibitor of cAMP transport by MRP4 and a promising adjunctive therapy to enhance GEM effectiveness in PDAC treatment.

Keywords: ABCC4/MRP4; Drug repositioning; Flurbiprofen; Gemcitabine resistance; Pancreatic ductal adenocarcinoma; cAMP.

MeSH terms

  • Anti-Inflammatory Agents, Non-Steroidal / pharmacology
  • Biological Transport / drug effects
  • Carcinoma, Pancreatic Ductal* / drug therapy
  • Carcinoma, Pancreatic Ductal* / metabolism
  • Carcinoma, Pancreatic Ductal* / pathology
  • Cell Line, Tumor
  • Cell Movement* / drug effects
  • Cell Proliferation* / drug effects
  • Cyclic AMP* / metabolism
  • Deoxycytidine* / analogs & derivatives
  • Deoxycytidine* / pharmacology
  • Drug Resistance, Neoplasm / drug effects
  • Drug Synergism
  • Flurbiprofen* / pharmacology
  • Gemcitabine*
  • Humans
  • Multidrug Resistance-Associated Proteins* / metabolism
  • Pancreatic Neoplasms / drug therapy
  • Pancreatic Neoplasms / metabolism
  • Pancreatic Neoplasms / pathology

Substances

  • Deoxycytidine
  • Multidrug Resistance-Associated Proteins
  • Gemcitabine
  • Cyclic AMP
  • ABCC4 protein, human
  • Flurbiprofen
  • Anti-Inflammatory Agents, Non-Steroidal