Molecular and Biochemical Characterization of Olive 4-Hydroxyphenyl Pyruvate Dioxygenase Involved in the Biosynthesis of Tocopherols Present in Virgin Olive Oil

J Agric Food Chem. 2024 Dec 25;72(51):28270-28279. doi: 10.1021/acs.jafc.4c06657. Epub 2024 Dec 12.

Abstract

Olive (Olea europaea) fruit contains high amounts of tocopherols that are responsible, along with secoiridoid phenolic compounds, for most of the antioxidant and anti-inflammatory properties of virgin olive oil. This study focuses on the molecular and biochemical characterization of olive 4-hydroxyphenyl pyruvate dioxygenase (OeHPPD) catalyzing the biosynthesis of homogentisic acid, which constitutes the phenolic residue in the tocopherol molecule. OeHPPD is a cytoplasmic enzyme with a molecular weight of 49.8 kDa and a predicted tertiary structure very similar to the Arabidopsis enzyme that suggests similar catalytic mechanisms. OeHPPD has an estimated Kcat of 75.26 s-1 and catalytic efficiency (Km/Kcat) of 0.145 μM-1 s-1 with 4-hydroxyphenyl pyruvate as the substrate. The expression analysis in fruits from selected olive cultivars harvested at different ripening stages indicates that the OeHPPD gene is temporally regulated and cultivar-dependent. Moreover, the analysis of OeHPPD expression in fruits affected by drought stress suggests that HPPD is involved in olive environmental adaptation.

Keywords: 4-hydroxyphenyl pyruvate dioxygenase; Olea europaea; olive oil; tocopherols.

MeSH terms

  • 4-Hydroxyphenylpyruvate Dioxygenase* / chemistry
  • 4-Hydroxyphenylpyruvate Dioxygenase* / genetics
  • 4-Hydroxyphenylpyruvate Dioxygenase* / metabolism
  • Fruit* / chemistry
  • Fruit* / enzymology
  • Fruit* / genetics
  • Fruit* / metabolism
  • Gene Expression Regulation, Plant
  • Kinetics
  • Molecular Weight
  • Olea* / chemistry
  • Olea* / enzymology
  • Olea* / genetics
  • Olea* / metabolism
  • Olive Oil* / chemistry
  • Olive Oil* / metabolism
  • Plant Proteins* / chemistry
  • Plant Proteins* / genetics
  • Plant Proteins* / metabolism
  • Tocopherols* / chemistry
  • Tocopherols* / metabolism

Substances

  • Olive Oil
  • Tocopherols
  • 4-Hydroxyphenylpyruvate Dioxygenase
  • Plant Proteins