Pharmacokinetics Integrated With Network Pharmacology to Investigate the Potential Mechanism of Lu-Jiao Fang Inhibited Endothelial-to-Mesenchymal Transition in Pressure Overload-Induced Cardiac Fibrosis

Biomed Chromatogr. 2025 Feb;39(2):e6075. doi: 10.1002/bmc.6075.

Abstract

The aim of this study was to investigate the potential mechanism of Lu-Jiao Fang (LJF) inhibiting endothelial-to-mesenchymal transition (EndMT) in pressure overload-induced cardiac fibrosis. Pharmacokinetic behaviors of the ingredients of LJF were evaluated by LC-MS/MS analysis. Then putative pathways by which LJF regulates EndMT were analyzed by network pharmacology and verified in transverse aortic constriction-induced cardiac fibrosis rats. Loganin, morroniside, salidroside, isopsoralen, and psoralen showed higher plasma, left and right ventricular Cmax and AUC0-t values than hesperidin, specnuezhenide, and icariside II. Twenty-four potential targets related to EndMT were identified, which were mainly involved in relaxin signaling pathway. AKT1, TP53, MMP9, HIF1A, Snail1, and MMP2 were key therapeutic targets in protein-protein interaction network. LJF reversed cardiac dysfunction, left ventricular dilation, and fibrosis and significantly downregulated collagen type I and III and EndMT regulators (Snail1 and Twist1) mRNA expression. In relaxin signaling pathway, the RXFP1 protein expression increased by 22.52%, and the protein phosphorylation of Smad2 and Smad3 decreased by 33.52% and 12.79%, in response to the treatment with LJF. This study initially revealed the EndMT inhibition effects and molecular mechanisms of LJF in cardiac fibrosis, providing a reference basis for the promotion of LJF in the clinic.

Keywords: Lu‐Jiao Fang; RXFP1 signaling; cardiac fibrosis; pharmacokinetics; pharmacology network.

MeSH terms

  • Animals
  • Chromatography, Liquid / methods
  • Drugs, Chinese Herbal* / pharmacokinetics
  • Drugs, Chinese Herbal* / pharmacology
  • Epithelial-Mesenchymal Transition* / drug effects
  • Fibrosis*
  • Male
  • Myocardium / metabolism
  • Myocardium / pathology
  • Network Pharmacology*
  • Protein Interaction Maps / drug effects
  • Rats
  • Rats, Sprague-Dawley*
  • Signal Transduction / drug effects
  • Tandem Mass Spectrometry / methods

Substances

  • Drugs, Chinese Herbal